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| ![]() MIL-D-70603(AR)
and finally with alcohol. The crucible and contents shall be dried
in an oven maintained at 60C. plus or minus 5C. for 30
minutes, cooled in a desiccator and weighed. The loss in weight
shall be calculated as the percentage of tetracene in the sample on
a dry basis as follows:
Tetracene, percent =
(C-D)1OO
W (1-.O1M)
Where:
=
c
weight of crucible and residue after extraction with
saturated ammonium acetate solution.
D=
weight of crucible and residue after treating with hot
water.
w=
weight of the sample.
moisture content of sample obtained from 4.3.3 in
M
=
percent.
The weight of the residue shall be
4.5.4.5 Antimony sulfide.
calculated from the determination of tetracene to percentage
antimony sulfide in the sample on a dry basis as follows:
(D-E) 100
Antimony sulfide, percent =
W (1-0.lM)
Where:
weight of crucible and sample after treating with hot
D
=
water .
E=
weight of crucible.
weight of the sample
w=
M=
moisture content of sample obtained from 4.3.3 in
percent.
4.5.4.6 Lead azide. The lead azide content in the sample on a
dry basis, shall be determined by subtracting from 100 the combined
percentages of barium nitrate, basic lead styphnate, tetracene and
antimony sulfide.
4.5.5 Functioning.
The detonator shall be assembled to the
4.5.5.1 Sensitivity.
applicable test fixture specified in 4.4.4, so that the firing pin
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